Analytical Chemistry of Synthetic Colorants by A. Whitaker (auth.), A. T. Peters, H. S. Freeman (eds.)

By A. Whitaker (auth.), A. T. Peters, H. S. Freeman (eds.)

More than one and a part many years have handed because the final ebook was once released describing advancements within the analytical chemistry of man-made colorants. within the intervening interval, the scope and technical features of instrumentation for analysing dyes and pigments has considerably improved. it really is now attainable to swiftly get to the bottom of a couple of difficulties whose recommendations have been formerly both unimaginable or very tough to accomplish. for example, the unambiguous project of the entire signs within the proton NMR spectrum of a trisazo direct dye, and the affirmation of the molecular weight of involatile, and, particularly, sulphonated dyes, with no derivatisation, at the moment are regimen analytical thoughts in lots of laboratories this day. moreover, it's now attainable to list the NMR spectrum of a dye molecule on under 1 mg of fabric, and we're not restricted to resolution spectra, seeing that stable samples can now be typically analysed in NMR experiments. when now not trying to be all encompassing, this quantity is meant to bridge the distance among what used to be lined within the prior paintings edited through Professor Venkataraman and the advancements that have considering that ensued in a few key components. It offers very important updates in X-ray crystallography, proton NMR, IR spectroscopy and mass spectrometry, and also covers subject matters akin to ESR, micro spectrophotometry and emission spectroscopy.

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L63 include a pattern for (30: R =anilino, R' =morpholino, M =Na) and confirm a pattern reported previouslyl66. Recent patterns for the two polymorphs, a and 13, of (30: R = o-toludino, R' = morpholino, M = Na)lfi7 also agree with those reported previouslyl68. However, in addition to these, there is a very comprehensive pattern available for an 'alpha-crystalline form' of the same compound l69 which does not agree with either of the patterns in the previous references. g. one could be an hydrate).

1. Acid Blue 324 is dimorphic213 , the forms being called 'old' and 'new'. The 'new' is obtained by heating a slurry of the 'old'. I. 1. 1. 71100) has been investigated four times 21 4-217. 215 agree 30 ANAL YTICAL CHEMISTRY OF SYNTHETIC COLORANTS that it is dimorphic, and both give traces of the two polymorphs that are very similar to each other. 2(} values of the P form, which are consistent with the form used as the pigment Bordeaux Red are given 215. 217 • A pattern is also available for CI.

I. I. D. R. V. S. Kozlova (1974) Fis. i khirniya tverd. , 1974 (5),33; (1975) Chern. , 83, 133460k. 78. A. Whitaker (1990) 1. Soc. Dyers C%urists, 106, 108. 79. A. Whitaker (1992) 1. Soc. Dyer Colourists, 108,282. 80. R. -J. -H. Molls and W. Gohrbandt (Bayer AG) (1973) DE 1,770,930. 81. K. Ruzicka and M. Kozlova (1984) CS 214,407. 82. R. -J. -H. Molls and W. Gohrbandt (Bayer AG) (1972) DE 1,770,931. 83. R. -J. -H. Molls and W. Gohrbandt (Bayer AG) (1977) DE 1,770,932. 84. Gosei Senryo Gijutsu Kenkyu Kumiai (1984) JP 59-11365; (1984) Chern.

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